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  Home > JCE Print > Journal of Chemical Education > Issues > 1995  > October  >
Laboratory Experiments
Synthesis and Variable-Temperature 1H NMR Conformational Analysis of Bis(eta5-cyclopentadienyl)titanium Pentasulfide: An Experiment for an Integrated, Advanced Laboratory Course
Anthony Diaz, Catherine Radzewich, and Mark Wicholas
Western Washington University, Bellingham, WA 98225
Cover
October 1995
Vol. 72 No. 10
p. 937
Abstract
The synthesis Of (eta5-C5H5)2TiS5 and the subsequent variable-temperature 1H NMR spectroscopy in d8-toluene form the basis for an integrated laboratory experiment combining inorganic and physical chemistry. The synthesis illustrates Schlenk techniques and use of a vacuum line, while the variable-temperature NMR spectroscopy follows the kinetics of the chair-to-chair inversion of the TiS5 ring.
More Information
*  Citation
 Diaz, Anthony; Radzewich, Catherine; Wicholas, Mark. J. Chem. Educ. 1995 72 937.
*  Keywords
*  History
 Created:
Last Updated:		 10/1/1999
5/22/2006
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