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  Home > JCE Print > Journal of Chemical Education > Issues > 1995  > October  >
Laboratory Experiments
Explorations in Organometallic Synthesis: Characterization and Structure Determinations of Binuclear Phosphine-Bridged Complexes of Platinum Using Multinuclear NMR and IR Spectroscopy.
Kimberly A. Brittingham and Serge Schreiner
Randolph-Macon College, Ashland, VA 23005

Thomas N. Gallaher
James Madison University, Harrisonburg, VA 22807

Cover
October 1995
Vol. 72 No. 10
p. 941
Abstract
A multi-step experiment has been developed for the inorganic chemistry laboratory in which students synthesize and characterize various bimetallic platinum complexes. Three 3-hr lab periods are required for the entire experimental/characterization process. Experimental techniques are not elaborate, but require the exclusion of oxygen with a nitrogen atmosphere as well as adequate hood ventilation. The isolated compounds are identified and characterized using infrared spectroscopy and multinuclear NMR.
More Information
*  Citation
 Brittingham, Kimberley A.; Schreiner, Serge; Gallagher, Thomas N. J. Chem. Educ. 1995 72 941.
*  Keywords
*  History
 Created:
Last Updated:		 10/1/1999
5/22/2006
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