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  Home > JCE Print > Journal of Chemical Education > Issues > 1996  > January  >
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The Microscale Laboratory
Air Stream-Assisted Sublimation on a Microscale: A Rapid Procedure Suitable for Sophomore Laboratory
Prem D. Sattsangi
Pennsylvania State University, Fayette Campus, Uniontown, PA 15401
Cover
January 1996
Vol. 73 No. 1
p. A3

Abstract
Using familiar apparatus, such as a 3-mL reaction vial, an air condenser, a stream of clean air/nitrogen/argon, an aluminum heating block and a hot plate, several compounds in the microscale amounts (50 mg), with its melting points ranging from 50-240 °C, have been successfully sublimed in 40 minutes.
More Information
*  Citation
Sattsangi, Prem D. J. Chem. Educ. 1996 73 A3.
*  Keywords
*  History
Created:
Last Updated:
9/25/1999
5/22/2006
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