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  Home > JCE Print > Journal of Chemical Education > Issues > 1996  > May  >
Features
The Microscale Laboratory
The Synthesis of 10-[Spiro[6,6]C60]-Anthrone: A Microscale Reaction of Fullerene
John Almy, Antonio Herrera, and Nazario Martín
Departamento de Quimica Organica 1, Universidad Complutense, E-28040, Madrid, Spain
Cover
May 1996
Vol. 73 No. 5
p. A105
Abstract
The microscale 1,3-dipolar cycloaddition reaction of Fullerene-C60 with 10-diazoanthrone leading to the methanofullerene adduct is described. The synthesis of the monoadduct and flash chromatography separation of the formed bisadducts was set up for two three hour laboratory periods.
More Information
*  Citation
 Almy, John; Herrera, Antonio; Martin, Nazario; Seoane, Carlos; Suzuki, Toshiyasu; Wudl, Fred. J. Chem. Educ. 1996 73 A105.
*  Keywords
*  History
 Created:
Last Updated:		 9/23/1999
5/22/2006
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