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  Home > JCE Print > Journal of Chemical Education > Issues > 1997  > July  >
In the Laboratory
Electrochemistry "Discovery" Course for Undergraduates
Michael Alan May and Vijay K. Gupta

Cover
July 1997
Vol. 74 No. 7
p. 824

Abstract
We developed a chemistry selected topics course at Central State University, "Introduction to Laboratory Techniques in Electrochemistry" to: (1) give undergraduates hands-on experience with electrochemical measurements, (2) prepare students for summer research in Fuel Cell and Battery technology. Since students "learn by doing", the course is suitable for undergraduates from sophomore to senior levels. Students complete 6 laboratories, based on a "less is more" philosophy which emphasizes analytic and creative process rather than mandatory topical coverage. Eight electrochemical experiments are available: Construction of Zinc-Copper battery stacks, Lead Acid Battery discharge-charge cycles, Conductimetric titration of aspirin with Ammonium Hydroxide, Ion Selective Electrode determination of Fluoride in water, Cyclic Voltammetry of Potassium Ferricyanide solution, Cyclic Voltammetry of Sulfuric acid on Platinum working electrode, Anodic Stripping Voltammetry of Lead ion in solution, Differential Pulse Polarography of Lead ion in solution. Topics discussed in lecture include: chemical definitions, electrical definitions, Oxidation-Reduction reactions, Electrochemical series, Electrodes, Electrochemical Cells, direct Coulometry, electrolysis, electrochemical process efficiency, equilibrium Potentiometry, real Cell Voltages, Ion Selective Electrode types and designs, reference electrode designs, working electrode materials, pH buffers, Cyclic Voltammetry, Anodic Stripping Voltammetry, Polarography, differential pulse Polarography, and simple electrochemical instrumentation circuits.
More Information
*  Citation
May, Michael Alan; Gupta, Vijay K. . J. Chem. Educ. 1997 74 824.
*  Keywords
Analytical Chemistry, Teaching/Learning Theory/Practice, Electrochemistry, Laboratory Instruction, Teaching/Learning Aids
*  History
Created:
Last Updated:
July 28, 1999
June 23, 2005
  Home > JCE Print > Journal of Chemical Education > Issues > 1997 > July > Page 824


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