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  Home > JCE Print > Journal of Chemical Education > Issues > 1997  > July  >
In the Laboratory
Removing Silicone Grease from Glassware
Thomas H. Lowry

Cover
July 1997
Vol. 74 No. 7
p. 841

Abstract
A recent note in this Journal (1) described the use of 5% aqueous hydrofluoric acid for removing silicone grease residues from round-bottom flasks. A safer and more convenient alternative is a saturated solution of sodium hydroxide in ethanol.

Caution: Eye protection must be worn at all times when handling solutions of sodium hydroxide. Avoid contact with skin and clothing. In case of contamination, wash affected areas thoroughly with water. Ethanol is flammable; use in a well-ventilated area away from sparks and flames.

The solution is readily prepared by warming sodium hydroxide pellets in 95% ethanol and is stored in a screw-cap polyethylene bottle. It is poured into the flask to be cleaned and heated on a steam cone or water bath for a few minutes, then returned to the storage bottle. The item being cleaned is rinsed thoroughly with water. No filtering is needed, and although the solution turns dark soon after being prepared, it can be kept indefinitely and used repeatedly without losing its effectiveness. It does not etch glass even after contact times of several hours and is an extremely effective general cleaning solution for glassware.

Literature Cited

1. Reilly, T. J. J. Chem. Educ. 1996, 73, 381.

More Information
*  Citation
Lowry, Thomas H. J. Chem. Educ. 1997 74 841.
*  Keywords
Laboratory Equipment/Apparatus, Solutions/Solvents
*  History
Created:
Last Updated:
July 28, 1999
June 23, 2005
  Home > JCE Print > Journal of Chemical Education > Issues > 1997 > July > Page 841


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