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  Home > JCE Print > Journal of Chemical Education > Issues > 1997  > July  >
In the Laboratory
A General Chemistry Experiment Incorporating Synthesis and Structural Determination
Hal Van Ryswyk
Cover
July 1997
Vol. 74 No. 7
p. 842
Abstract
An experiment for the general chemistry laboratory is described wherein gas chromatography-mass spectroscopy (GC-MS) and diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) are used to characterize the products of a series of microscale reactions on vanillin. A single sophisticated instrument can be incorporated into the laboratory given sufficient attention to the use of sampling accessories and software macros. Synthetic experiments coupled with modern instrumental techniques can be used in the general chemistry laboratory to illustrate the concepts of synthesis, structure, bonding, and spectroscopy.
More Information
*  Citation
 Van Ryswyk, Hal. J. Chem. Educ. 1997 74 842.
*  Keywords
 Laboratory Instruction, Introductory/High School Chemistry, Instrumental Methods, Microscale, Organic Synthesis, Spectroscopy
*  History
 Created:
Last Updated:		 July 28, 1999
June 23, 2005
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