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McGraw-Hill: New York, 1996. xii + 778 pp. ISBN 0-07-057074-4.
Experiments in Physical Chemistry has long been one of the best textbooks available for undergraduate courses in physical chemistry laboratory. The present edition
follows a similar format as previous editions, consisting of (i) a
series of introductory sections dealing with common
aspects of all experiments, such as recording of data, report
writing, data and error analysis, and the use of computer
software to aide in these, (ii) 48 experiments spanning 12
fundamental areas, and (iii) a series of resource chapters
providing an introduction to electronics, instruments,
techniques, and procedures commonly utilized in the
performance of experiments in physical chemistry. Some
needed changes have been incorporated in this edition, most
notably the addition of sections that recognize the increased
role of computers in modern experimentation. In particular,
the section on computer software has been expanded and
moved ahead of the experiments. The use of word
processing, spreadsheets, and symbolic mathematics programs is
emphasized, with examples using some of the most
popular commercial programs. Three new experiments have
been added and a fourth substantially modified. Each of the
44 other experiments has undergone some review and
modernization, and a much-needed section on safety issues
has been added to each. A resource chapter on computer
interfacing, treating data types, programming languages and
interfacing has been added. Examples are given for
programming RS-232 communication and analog/digital
interface boards using visual basic routines.
I recommend this book be given serious
consideration as a text for a one- or two-semester course in physical
chemistry laboratory. The approach to experimentation in
physical chemistry, the experiments, and the techniques that
are described can form a solid basis for such a course. My
one criticism is that the text offers only a limited number of
laser-based experiments. This represents a minor drawback
to an overall strong text, since those who wish to
emphasize the use of lasers can easily supplement the choice
of experiments from the numerous alternatives available
in the literature.
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