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  Home > JCE Print > Journal of Chemical Education > Issues > 1997  > May  >
In the Laboratory
The Phase-Transfer Catalyzed Preparation of Mo(CO)4(dphos): An Intermediate-Level Organometallic-Inorganic Experiment
James A. S. Howell
Chemistry Department, University of Keele, Staffordshire, UK, ST55BG
Cover
May 1997
Vol. 74 No. 5
p. 577
Abstract
Mo(CO)4(diphos) may be prepared by the phase transfer catalysed substitution of Mo(CO)6 with diphos in the presence of Bu4NI. The complex may be characterised by infrared and 1H and 13C NMR spectroscopy.
More Information
*  Citation
 Howell, James A. S. J. Chem. Educ. 1997 74 577.
*  Keywords
 Inorganic Chemistry, Organometallics, Metal Carbonyls, Spectroscopy, Molybdenum
*  History
 Created:
Last Updated:		 July 28, 1999
June 23, 2005
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