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  Home > JCE Print > Journal of Chemical Education > Issues > 1997  > November  >
In the Laboratory
The Microscale Laboratory
A Convinient Procedure for Microscale Bezoylations
Sangeeta Pandita and Samta Goyla
Zakir Husain College, Department of Chemistry, J. L. Nehru Marg, New Delhi 110002, India

Cover
November 1997
Vol. 74 No. 11
p. 1335

Abstract
Benzoylation by the Schotten - Baumann method is a useful way to identify and characterize aromatic amines, phenols, sugars, etc. However, for best results, the method requires vigorous shaking in well-stoppered vessels with dropwise addition of benzoyl chloride (1). The fact that benzoyl chloride is a lachrymator may require that these reactions be done outside the laboratory environment in open areas. We report here a convenient procedure for the microscale benzoylation of aromatic amines and phenols.
More Information
*  Citation
Pandita, Sangeeta; Goyla, Samta. J. Chem. Educ. 1997 74 1335.
*  Keywords
Microscale and Organic Chemistry
*  History
Created:
Last Updated:
July 26, 1999
June 23, 2005
  Home > JCE Print > Journal of Chemical Education > Issues > 1997 > November > Page 1335


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