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  Home > JCE Print > Journal of Chemical Education > Issues > 1999  > May  >
In the Laboratory
Synthesis of a 7-Oxanorbornene Monomer: A Two-Step Sequence Preparation for the Organic Laboratory
Marcia B. France, Lisa T. Alty, and T. Markley Earl
Washington and Lee University, Department of Chemistry, Lexington, VA 24450
Cover
May 1999
Vol. 76 No. 5
p. 659
Abstract
We have developed a two-step synthetic sequence for our introductory organic laboratory that demonstrates key reactions that the students learn concurrently in the lecture portion of their organic chemistry course. It represents the Diels-Alder reaction and solvolysis of an anhydride accompanied by Fischer esterification. Both of these steps produce crystals in a dramatic manner that catches the students' attention. This sequence can stand on its own as part of an organic laboratory, or the product can be utilized as a monomer for ring-opening metathesis polymerization (ROMP) studies.
More Information
*  Citation
 France, Marcia B.; Alty, Lisa T.; Earl, T. Markley. J. Chem. Educ. 1999 76 659.
*  Keywords
 Laboratory Instruction; Organic Chemistry; Synthesis; NMR Spectrometry; Organic Synthesis
*  History
 Created:
Last Updated:		 June 11, 1999
June 23, 2005
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