Data from multiple analytical methods are often required to identify or characterize samples. Typical undergraduate experiments utilize only one or two techniques in a given experiment. This paper describes a novel experiment that requires students to obtain and interpret data from several analytical techniques to identify the brand name of a commercial antacid. Students receive a ground sample of a commercial antacid. They are required to design a set of experiments utilizing computer controlled titrations (CCT), atomic absorption (AA), gas chromatography-mass spectroscopy (GCMS), and careful quantitative manual titrations using a visual indicator of their choice to determine the brand name of their sample from a list of six to eight choices.
Supplement
A list of equipment and chemicals, instructor's notes for student handouts and general hints, and a handout for students describing the application experiment and its write-up are provided.
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