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  Home > JCE Print > Journal of Chemical Education > Issues > 1999  > March  >
In the Laboratory
Synthesis of Molybdenum-Molybdenum Quadruple Bonds: A Multistep Advanced Synthesis Laboratory Experiment
Laura E. Pence, Amy M. Weisgerber, and Florence A. Maounis
Department of Chemistry, University of Hartford, West Hartford, CT 06117
Cover
March 1999
Vol. 76 No. 3
p. 404
Abstract
An advanced synthetic inorganic experiment is described in which students prepare Mo2(O2CCH3)4, a species containing a quadruple metal-metal bond. They then study the ligand substitution chemistry of the compound to form the unbridged systems [Mo2Cl8]4- and resources.
Supplement
A detailed version of the laboratory experiment is available as supplementary material. The text can be accessed as Microsoft Word documents and the figures as Adobe Illustrator and photoshop files. This material has been compressed into sit (for Macintosh) and zip (for Windows)files. The material can also be accessed as a pdf file using Acrobat Reader.
*  Contents
*  Download
supp404.pdf

supp404.sit

supp404.zip
More Information
*  Citation
 Pence, Laura E.; Weisgerber, Amy M.; Maounis, Florence A. J. Chem. Educ. 1999 76 404.
*  Keywords
 Inorganic Chemistry; Laboratory Instruction; Coordination Chemistry; Synthesis; Transition Elements; Inorganic Synthesis
*  History
 Created:
Last Updated:		 June 15, 1999
November 22, 2005
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