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In under 600 pages, the authors introduce the reader
to more than 150 NMR experiments and give some sense
of the depth possible for each experiment. While the book
is titled Basic NMR Experiments, most readers would
consider these experiments as some of the most sophisticated a
chemist who is not an NMR expert would consider doing. With
these comments in mind, let me speak to the strengths and
potential uses of the book.
This book is not for the novice NMR spectroscopist
who has never run anything but a "normal" proton
spectrum. Although it starts with a section on shimming the
magnets and on routine tests like sensitivity, the detail available on
more sophisticated multipulse sequences or 2-D spectroscopy
is not sufficient for a novice to run these sequences with
comfort. However, for a person like me who has run some simple 2D
sequences like COSY or HETCOR and who has some sense
of the power of other sequences, the book is great. It
collects in one place all the common pulse sequences, including
those using pulsed field gradients. I feel as though most
of the instruction I received when our high-field NMR was
installed is contained in this book, making it a much more
useful resource than my scribbled notes. In addition to 2-D
experiments, the book includes brief descriptions of
decoupling techniques, dynamic NMR spectroscopy, experiments
with chiral shift reagents, and even 3-D experiments and solid
state NMR spectroscopy. Of particular value is the
identification in each experiment of other experiments giving basically
the same information. When used along with the indication of
the time required for each experiment, it is possible to
decide which is the most efficient experiment to elicit certain types
of information. In addition, the discussion of each
experiment illuminates the experiment's "warts", such as poor
signal-to-noise ratio or the need for long relaxation times.
I think this is a great book, when considered as an
encyclopedia of the techniques a modern NMR
spectroscopist might need. While new pulse sequences continue to be
developed, this book will be a useful resource for the next
five years, at least.
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