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  Home > JCE Print > Journal of Chemical Education > Issues > 2000  > March  >
In the Laboratory
Microwave Irradiation Reactions: Synthesis of Analgesic Drugs
Gholam A. Mirafzal and Jolene M Summer
Department of Chemistry, Drake University, Des Moines, IA 50311
Cover
March 2000
Vol. 77 No. 3
p. 356
Abstract
Over-the-counter analgesics such as aspirin, acetanilide, phenacetin, and acetaminophen are conveniently prepared in a microwave at 30% power for five minutes. Recrystallization from appropriate solvents results in solid products in good to excellent yields. Melting points, thin layer chromatography, and infrared spectroscopy all confirm that the products are pure.
More Information
*  Citation
 Mirafzal, Gholam A.; Summer, Jolene M. J. Chem. Educ. 2000 77 356.
*  Keywords
 Organic Chemistry; Laboratory Instruction; microwave; Drugs / Pharmaceuticals
*  History
 Created:
Last Updated:		 February 14, 2000
April 15, 2005
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