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  Home > JCE Print > Journal of Chemical Education > Issues > 2000  > May  >
In the Laboratory
Self-Assembly of Microporous Thiogermanate Frameworks
Mark J. MacLachlan, Robert W. J. Scott, Geoffrey A. Ozin, and Douglas F. McIntosh
Department of Chemistry, University of Toronto, Toronto, ON M5S 3H6, Canada
Cover
May 2000
Vol. 77 No. 5
p. 630
Abstract
A safe undergraduate laboratory experiment involving the synthesis of microporous metal germanium sulfide materials under aqueous, room-temperature conditions is described. It introduces students to the synthetic methods of self-assembly and solid-state chemistry. The products are characterized by powder X-ray diffraction and vibrational spectroscopy.
Supplement
Demonstrator notes, answers to lab questions, and figures are included.
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*  Citation
 MacLachlan, Mark J.; Scott, Robert W. J.; Ozin, Geoffrey A.; McIntosh, Douglas F. J. Chem. Educ. 2000 77 630.
*  Keywords
 Germanium; Inorganic Chemistry; Laboratory Instruction; Solid-State Chemistry; Sulfur
*  History
 Created:
Last Updated:		 March 31, 2000
August 31, 2005
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