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  Home > JCE Print > Journal of Chemical Education > Issues > 2002  > April  >
In the Laboratory
129Xe NMR of Zeolite NaY in the Inorganic Chemistry Laboratory
Tanja Pietraß
Department of Chemistry, New Mexico Tech, Socorro, NM 87801
Cover
April 2002
Vol. 79 No. 4
p. 492
Abstract
129Xe NMR spectroscopy of xenon physisorbed in commercially available zeolite NaY is introduced as an experiment suitable for the inorganic chemistry laboratory in the senior year. The integration of concepts from inorganic and physical chemistry (ideal gas law, gas adsorption, solid state structure, porous materials, NMR spectroscopy) make this experiment also suitable for an integrated laboratory approach. The chemical shift of 129Xe at different loadings in the a- cages of zeolite NaY is used to derive the intrinsic chemical shift by extrapolation to zero loading.
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*  Citation
 Pietraß, Tanja. J. Chem. Educ. 2002 79 492.
*  Keywords
 Gases; Inorganic Chemistry; Laboratory Instruction; NMR Spectrometry; Physical Chemistry
*  History
 Created:
Last Updated:		 March 1, 2002
March 16, 2005
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