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  Home > JCE Print > Journal of Chemical Education > Issues > 2004  > July  >
In the Laboratory
Simple Epoxide Formation for the Organic Laboratory Using Oxone
William C. Broshears, John J. Esteb, Jeremy Richter, and Anne M. Wilson
Department of Chemistry, Butler University, Indianapolis, IN 46208
Cover
July 2004
Vol. 81 No. 7
p. 1018
Abstract
We present an epoxide formation experiment for a second-semester organic chemistry laboratory. This oxidation utilizes Oxone, a commercially available oxidizing agent, in the industrially relevant process of epoxide formation. The oxidant performing the oxidation is dimethyldioxirane, which is formed in situ. This experiment demonstrates a simple synthesis of an epoxide and formation of a secondary oxidizing agent.
Supplement
Instructions for the students, laboratory questions, notes for the instructor, and safety information are available.
*  Contents JCE2004p1018W.doc (Microsoft Word)
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*  Citation
 Broshears, William C.; Esteb, John J.; Richter, Jeremy; Wilson, Anne M. J. Chem. Educ. 2004 81 1018.
*  Keywords
 Laboratory Instruction; Organic Chemistry; Organic Synthesis
*  History
 Created:
Last Updated:		 May 27, 2004
January 19, 2005
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