One principle of green chemistry is the elimination of waste in chemical processes prior to its generation. For this dry laboratory, a procedure for the nitrosation of 2,5-hexanedione is evaluated using a recently described metrics system. Since the reaction conditions for the synthesis of 3-acetyl-5-methylisoxazole are solvent-free and the process utilizes catalytic chemistry, this experiment concentrates on an analysis of the impact of auxiliary substances such as extraction solvents and separation agents as sources of waste in chemical processes. The importance of yield improvement as it relates to waste minimization is also highlighted.
Supplement
Uses and other preparations for 3-acetyl-5-methylisoxazole, the procedure for the environmental-impact analysis, and student exercises are available.
Our Secondary School editors work hard to distill all the JCE materials to produce a fraction of particular interest to high school teachers. We call it CLIC.
In recent years we have worked hard to better match our advertisers with our readers. When shopping for chemistry education materials, visit our advertisers' WWW sites first.
Take JCE along on your outreach missions. Copies of the Journal, guest access to JCE Online, our publications catalog, and more are available for your participants.