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  Home > JCE Print > Journal of Chemical Education > Issues > 2005  > October  >
In the Laboratory
The Incorporation of Single Crystal X-ray Diffraction into the Undergraduate Chemistry Curriculum Using Internet-Facilitated Remote Diffractometer Control
P. S. Szalay
Department of Chemistry, Muskingum College, New Concord, OH 43762

M. Zeller and A. D. Hunter
Department of Chemistry, Youngstown State University, Youngstown, OH 44555

Cover
October 2005
Vol. 82 No. 10
p. 1555

Abstract
A laboratory experiment on single crystal X-ray diffraction has been developed and implemented in an inorganic chemistry course for undergraduate students via Internet-facilitated remote diffractometer control. The experiment was carried out from a remote location, a computer lab at Muskingum College, with the X-ray diffractometer being housed at Youngstown State University. In this experiment, the structure of (η6-p-fluoroaniline)chromium(tricarbonyl) was determined as a representative example.
Supplement
Details of each of the experimental stages and alternative options, copies of the student handouts, and a presentation developed by A. D. Hunter that covers some of the basics of crystallography are available.
*  Download
JCE2005p1555W.pdf

More Information
*  Citation
Szalay, P. S.; Hunter, A. D.; Zeller, M. J. Chem. Educ. 2005 82 1555.
*  Keywords
Computer-Based Learning; Coordination Compounds; Crystals / Crystallography; Hands-On Learning / Manipulatives; Inorganic Chemistry; Internet / Web-Based Learning; Laboratory Instruction; Physical Chemistry; Second-Year Undergraduate; Transition Elements; Upper-Division Undergraduate; X-ray Crystallography
*  History
Created:
Last Updated:
August 30, 2005
September 9, 2005
  Home > JCE Print > Journal of Chemical Education > Issues > 2005  > October  > Page 1555


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