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  Home > JCE Print > Journal of Chemical Education > Issues > 2006  > February  >
In the Laboratory
Determination of the Heat of Combustion of Biodiesel Using Bomb Calorimetry. A Multidisciplinary Undergraduate Chemistry Experiment
Stephen M. Akers, Jeremy L. Conkle, Stephanie N. Thomas, and Keith B. Rider
Department of Natural Sciences, Longwood University, Farmville, VA 23909

Cover
February 2006
Vol. 83 No. 2
p. 260

Abstract
An integrated undergraduate laboratory activity involving the synthesis and characterization of a diesel fuel substitute, biodiesel, is presented. Biodiesel is currently a popular topic in the field of green chemistry because it is a non-petroleum fuel that can be efficiently produced from waste vegetable oil. As a fuel, it requires no engine modifications and results in lower pollution emissions including carcinogens and carbon dioxide. Over a three-week period, students synthesize biodiesel, measure its heat of combustion, density, and cloud point, then compare these properties to conventional petroleum diesel. Heats of combustion are measured in a common laboratory bomb calorimeter and cloud point is measured using a UV–vis spectrophotometer.
Supplement
Instructions for the student, a three-week timetable for the experiment, and notes to the instructor are available.
*  Contents Folder JCE2006p0260W containing JCE2006p0260W_1.doc and JCE2006p0260W_2.doc (Microsoft Word)
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JCE2006p0260W.pdf

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More Information
*  Citation
Akers, Stephen M.; Conkle, Jeremy L.; Thomas, Stephanie N.; Rider, Keith B. J. Chem. Educ. 2006 83 260.
*  Keywords
Calorimetry / Thermochemistry; Environmental Chemistry; Esters; Green Chemistry; Hands-On Learning / Manipulatives; Interdisciplinary / Multidisciplinary; Laboratory Instruction; Lipids; Organic Chemistry; Physical Chemistry; Thermodynamics; Upper-Division Undergraduate; UV-Vis Spectroscopy
*  History
Created:
Last Updated:
1/5/2006
1/9/2006
  Home > JCE Print > Journal of Chemical Education > Issues > 2006  > February  > Page 260


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