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| Home > JCE Print > Journal of Chemical Education > Issues >
2006
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February
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In the Laboratory
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Determination of the Heat of Combustion of Biodiesel Using Bomb Calorimetry. A Multidisciplinary Undergraduate Chemistry Experiment
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Stephen M. Akers, Jeremy L. Conkle, Stephanie N. Thomas, and Keith B. Rider
Department of Natural Sciences, Longwood University, Farmville, VA 23909
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February 2006 Vol. 83 No. 2 p. 260
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| Abstract |
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An integrated undergraduate laboratory activity involving the synthesis and characterization of a diesel fuel substitute, biodiesel, is presented. Biodiesel is currently a popular topic in the field of green chemistry because it is a non-petroleum fuel that can be efficiently produced from waste vegetable oil. As a fuel, it requires no engine modifications and results in lower pollution emissions including carcinogens and carbon dioxide. Over a three-week period, students synthesize biodiesel, measure its heat of combustion, density, and cloud point, then compare these properties to conventional petroleum diesel. Heats of combustion are measured in a common laboratory bomb calorimeter and cloud point is measured using a UV–vis spectrophotometer.
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| Supplement |
Instructions for the student, a three-week timetable for the experiment, and notes to the instructor are available.
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Contents |
Folder JCE2006p0260W containing JCE2006p0260W_1.doc and JCE2006p0260W_2.doc (Microsoft Word)
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Download |
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| More Information |
 Citation
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Akers, Stephen M.; Conkle, Jeremy L.; Thomas, Stephanie N.; Rider, Keith B. J. Chem. Educ. 2006 83 260.
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 Keywords
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Calorimetry / Thermochemistry; Environmental Chemistry; Esters; Green Chemistry; Hands-On Learning / Manipulatives; Interdisciplinary / Multidisciplinary; Laboratory Instruction; Lipids; Organic Chemistry; Physical Chemistry; Thermodynamics; Upper-Division Undergraduate; UV-Vis Spectroscopy
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 History
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Created:
Last Updated: |
1/5/2006
1/9/2006
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| Home > JCE Print > Journal of Chemical Education > Issues >
2006
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February
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260
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