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  Home > JCE Print > Journal of Chemical Education > Issues > 2008  > June  >
In the Laboratory
The Microscale Laboratory
A Safe and Efficient Technique for the Production of HCl/DCl Gas
Steven G. Mayer, Raymond R. Bard, and Kevin Cantrell
Department of Chemistry, University of Portland, Portland, OR 97203
Cover
June 2008
Vol. 85 No. 6
p. 847
Abstract
We present a safe and efficient technique to generate HCl/DCl gas for use in the classic physical chemistry experiment that introduces students to ro-vibrational spectroscopy. The reaction involves thionyl chloride and a mixture of water and deuterium oxide to produce HCl/DCl gas with SO2 gas as a byproduct. The entire reaction is carried out in a microscale apparatus at atmospheric pressure.
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More Information
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Citation
Mayer, Steven G.; Bard, Raymond R.; Cantrell, Kevin. J. Chem. Educ. 2008, 85, 847.
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Keywords
Gases; Hands-On Learning / Manipulatives; IR Spectroscopy; Microscale Lab; Physical Chemistry; Upper-Division Undergraduate
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History
Created:
Last Updated:
5/5/2008
5/7/2008
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