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  Home > JCE Print > Journal of Chemical Education > Issues > 2001  > October  >
In the Laboratory
Moisture Analysis in Lotion by Karl Fischer Coulometry. An Experiment for Introductory Analytical Chemistry
Patricia Ann Mabrouk and Kristine Castriotta
Department of Chemistry, Northeastern University, Boston, MA 02115

Cover
October 2001
Vol. 78 No. 10
p. 1385

Abstract

This paper describes an experiment that can be used in an introductory analytical chemistry laboratory course. It allows the student analyst to measure the moisture content of various hand and body lotions using the coulometric Karl Fischer (KF) technique, providing a modern alternative to the traditional electrochemical experiments usually explored in introductory analytical chemistry courses. The experiment introduces students to an important technique in industry and commerce, which is highly sensitive, accurate, and precise, and which can be used to study a wide range of samples. The measurement times are short, allowing students to experience the analytical problem-solving process from start to finish in a single 3-hour laboratory period. One KF coulometer can adequately service even a large analytical chemistry class (>80 students). In spring 2000, students identified the KF experiment as the most popular, most useful, and most educational experiment in our analytical chemistry laboratory curriculum.

Supplement
Prelab questions, detailed instructions for the experimental procedure, a discussion of hazards, and notes for TAs are available.
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More Information
*  Citation
Mabrouk, Patricia Ann; Castriotta, Kristine. J. Chem. Educ. 2001 78 1385.
*  Keywords
Analytical Chemistry; Consumer Chemistry; Electrochemistry; Laboratory Instruction; Quantitative Analysis; Redox Reactions
*  History
Created:
Last Updated:
September 13, 2001
August 31, 2005
  Home > JCE Print > Journal of Chemical Education > Issues > 2001  > October  > Page 1385


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