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  Home > JCE Print > Journal of Chemical Education > Issues > 1998  > January  >
In the Laboratory
Notes on Converting to Microscale
Antonio Herrera and John Almy
CSU Stanislaus, Chemistry Department, 801 W. Monte Vista Avenue, Turlock, CA 95382
Cover
January 1998
Vol. 75 No. 1
p. 83
Abstract
As a substitute for commercial microscale glassware kits, common glassware items have been utilized to carry out techniques such as refluxing, recrystallization, elution chromatography, extractions and boiling point determinations. In addition four microscale experiments are described which do not require kits: synthesis of 4,6,8-trimethylazulene, isolation of cholesterol by continuous extraction, synthesis of benzoic acid via a Grignard reaction and synthesis of meso-tetraphenylporphyrin.
More Information
*  Citation
 Herrera , Antonio; Almy, John. J. Chem. Educ. 1998 75 83.
*  Keywords
 Organic Chemistry, Laboratory Instruction, Laboratory Equipment/Apparatus, and Microscale
*  History
 Created:
Last Updated:		 June 28, 1999
June 23, 2005
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